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Beilstein J. Org. Chem. 2006, 2, No. 4, doi:10.1186/1860-5397-2-4
Graphical Abstract
Scheme 1: Synthesis of phosphorothioates using microwave irradiation
Scheme 2: Ambident nucleophile ammonium O,O'-diethylthiophosphate
Scheme 3: Synthesis of ammonium O,O'-diethyl thiophosphate
Scheme 4: Solvent and leaving group effects on the synthesis phosphorothioates
Scheme 5: Reaction of ammonium O,O'-diethyl thiophosphate with benzoyl chloride
Scheme 6: Reaction of triethylammonium O,O'-diethyl thiophosphate with benzoyl chloride
Scheme 7: Synthesis of phosphorothioates using triethylammonium O,O'-diethyl thiophosphate using microwave ir...